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Utilizing a unique flow-through photochemical reactor capable of subjecting the samples to deep-UV (185 nm) radiation, generation efficiency was found to be independent of whether Sb(III), Sb(V), or organometallic species [trimethyltantimony(V)dibromine, TMSb(V)] were present, eliminating the shortcoming of Sb species depended sensitivity encountered during direct solution nebulization by ICPMS. Furthermore, the potentially severe matrix effect from seawater was efficiently eliminated by using a mixture of 5% (v/v) formic and 15% acetic acids (v/v) as the photochemical reductant, making direct determination of Sb in seawater feasible. The proposed method provides a 15-fold improvement in sensitivity over direct solution nebulization. A method detection limit of 0.0006 ng g-1 based on external calibration was obtained (0.0002 ng g-1 for isotope dilution), yielding a 15-fold improvement over that for direct solution nebulization. Accuracy is demonstrated by analysis of two water certified reference materials (CRMs, e.g., SLRS-6 and NIST 1640a) with satisfying results. In addition, spike recoveries of 100.6 ± 5.5% and 100.8 ± 3.8% (standard deviation, n = 3) were obtained for NASS-6 and CASS-5 seawater CRMs, respectively, since no certified values for Sb has been established for these materials. The performance of several calibration strategies, including double isotope dilution (ID), multiple and single-point gravimetric standard additions with internal standardization, as well as multiple and single-point gravimetric standard additions alone was examined. High precision of determination of Sb in four natural water samples (0.51-1.4%) was realized based on ID calibration, whereas one-point gravimetric standard addition calibration with internal standardization provided precisions of 1.6% and 3.3% at 0.22 and 0.44 ng g-1 levels, respectively, in seawater. © 2015 American Chemical Society.", "keywords" : [ { "otype" : "Keyword", "mtid" : 496, "link" : "/api/keyword/496", "label" : "STANDARDIZATION", "published" : true, "oldId" : 496, "snippet" : true }, { "otype" : "Keyword", "mtid" : 4945, "link" : "/api/keyword/4945", "label" : "Seawater", "published" : true, "oldId" : 4945, "snippet" : true }, { "otype" : "Keyword", "mtid" : 6303, "link" : "/api/keyword/6303", "label" : "CALIBRATION", "published" : true, "oldId" : 6303, "snippet" : true }, { "otype" : "Keyword", "mtid" : 7769, "link" : "/api/keyword/7769", "label" : "Mass spectrometry", "published" : true, "oldId" : 7769, "snippet" : true }, { "otype" : "Keyword", "mtid" : 8182, "link" : "/api/keyword/8182", "label" : "ISOTOPES", "published" : true, "oldId" : 8182, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1000357, "link" : "/api/keyword/1000357", "label" : "external calibration", "published" : true, "oldId" : 1000357, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1011288, "link" : "/api/keyword/1011288", "label" : "Mass spectrometers", "published" : true, "oldId" : 1011288, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1017231, "link" : "/api/keyword/1017231", "label" : "inductively coupled plasma mass spectrometry", "published" : true, "oldId" : 1017231, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1022494, "link" : "/api/keyword/1022494", "label" : "water analysis", "published" : true, "oldId" : 1022494, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1029740, "link" : "/api/keyword/1029740", "label" : "Organometallics", "published" : true, "oldId" : 1029740, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1119065, "link" : "/api/keyword/1119065", "label" : "Certified reference materials", "published" : true, "oldId" : 1119065, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1549016, "link" : "/api/keyword/1549016", "label" : "Standard addition calibration", "published" : true, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1549092, "link" : "/api/keyword/1549092", "label" : "Inductively coupled plasma mass spectrometries (ICPMS)", "published" : true, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1549098, "link" : "/api/keyword/1549098", "label" : "Internal standardization", "published" : true, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1549099, "link" : "/api/keyword/1549099", "label" : "Method detection limits", "published" : true, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1549107, "link" : "/api/keyword/1549107", "label" : "Seawater effects", "published" : true, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1549108, "link" : "/api/keyword/1549108", "label" : "Natural water samples", "published" : true, "snippet" : true }, { "otype" : "Keyword", "mtid" : 1549109, "link" : "/api/keyword/1549109", "label" : "Photochemical reactor", "published" : true, "snippet" : true } ], "digital" : null, "printed" : null, "sourceYear" : 2019, "foreignEdition" : true, "foreignLanguage" : true, "fullPublication" : true, "conferencePublication" : false, "nationalOrigin" : null, "missingAuthor" : false, "oaType" : "NONE", "oaCheckDate" : "2024-03-02", "oaFree" : false, "citationCount" : 48, "citationCountUnpublished" : 0, "citationCountWoOther" : 48, "independentCitCountWoOther" : 27, "nationalOriginCitationCount" : 0, "foreignEditionCitationCount" : 48, "doiCitationCount" : 45, "wosCitationCount" : 48, "scopusCitationCount" : 22, "wosScopusCitationCount" : 48, "wosScopusCitationCountWoOther" : 48, "wosScopusIndependentCitationCount" : 27, "wosScopusIndependentCitationCountWoOther" : 27, "independentCitationCount" : 27, "selfCitationCount" : 21, "unhandledCitationCount" : 0, "citingPubCount" : 48, "independentCitingPubCount" : 27, "citingPubCountWoOther" : 48, "independentCitingPubCountWoOther" : 27, "unhandledCitingPubCount" : 0, "citedPubCount" : 5, "citedCount" : 5, "ratings" : [ { "otype" : "MtaRating", "mtid" : 11435012, "link" : "/api/mtarating/11435012", "label" : "X. 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