TY - JOUR AU - Abrankó, László AU - Jókainé Szatura, Zsuzsa AU - Fodor, Péter TI - Investigation of the species-specific degradation behaviour of methylmercury and ethylmercury under microwave irradiation JF - ANALYTICAL AND BIOANALYTICAL CHEMISTRY J2 - ANAL BIOANAL CHEM VL - 383 PY - 2005 IS - 3 SP - 448 EP - 453 PG - 6 SN - 1618-2642 DO - 10.1007/s00216-005-3395-x UR - https://m2.mtmt.hu/api/publication/1390068 ID - 1390068 AB - The degradation behaviour of methylmercury (MeHg) under microwave irradiation is investigated, as is the (different) degradation behaviour of ethylmercury (EtHg) under similar irradiation. A simple and highly sensitive SPME-GC-pyrolysis-AFS system was used to analyse the aqueous MeHg and EtHg standard solutions after derivatization with sodium tetraphenylborate (NaBPh4). Samples were irradiated in a microwave digester at microwave powers ranging from 20 to 160 W for durations of 2 to 10 min. The different tolerances towards microwave treatment of the two organomercury species were evident. Practically no degradation was experienced for MeHg for up to 8 minutes of irradiation at 120 W or for up to 4 minutes at 160 W. Significant analyte loss was observed for EtHg after 2 minutes at 40 W of microwave power. LA - English DB - MTMT ER - TY - JOUR AU - Ipolyi, I AU - Massanisso, P AU - Sposato, S AU - Fodor, Péter AU - Morabito, R TI - Concentration levels of total and methylmercury in mussel samples collected along the coasts of Sardinia Islands (Italy) JF - ANALYTICA CHIMICA ACTA J2 - ANAL CHIM ACTA VL - 505 PY - 2004 IS - 1 SP - 145 EP - 151 PG - 7 SN - 0003-2670 DO - 10.1016/S0003-2670(03)00174-0 UR - https://m2.mtmt.hu/api/publication/1719946 ID - 1719946 LA - English DB - MTMT ER - TY - JOUR AU - Leermakers, M AU - Nguyen, HL AU - Kurunczi, Sándor AU - Vanneste, B AU - Galletti, S AU - Baeyens, W TI - Determination of methylmercury in environmental samples using static headspace gas chromatography and atomic fluorescence detection after aqueous phase ethylation JF - ANALYTICAL AND BIOANALYTICAL CHEMISTRY J2 - ANAL BIOANAL CHEM VL - 377 PY - 2003 SP - 327 EP - 333 PG - 7 SN - 1618-2642 DO - 10.1007/s00216-003-2116-6 UR - https://m2.mtmt.hu/api/publication/137604 ID - 137604 LA - English DB - MTMT ER -