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<div class="JournalArticle Publication short-list"> <div class="authors"> <span class="author-name" > Lengyel, Zs ✉ </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10028688"> <a href="/gui2/?type=authors&mode=browse&sel=10028688" target="_blank">Lukács, A</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10028691"> <a href="/gui2/?type=authors&mode=browse&sel=10028691" target="_blank">Szabó, A</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10010104"> <a href="/gui2/?type=authors&mode=browse&sel=10010104" target="_blank">Nagymajtényi, L</a> </span> <span class="author-type"> </span> </div ><div class="title"><a href="/gui2/?mode=browse¶ms=publication;1919903" mtid="1919903" target="_blank">General toxicity and neurotoxicity of lead and mercury, in combination with dimethoate, in rats after subchronic oral exposure.</a></div> <div class="pub-info"> <span class="journal-title">TRACE ELEMENTS AND ELECTROLYTES</span> <span class="journal-volume">23</span> : <span class="journal-issue">4</span> <span class="page"> pp. 242-246. , 5 p. </span> <span class="year">(2006)</span> </div> <div class="pub-end"><div class="identifier-list"> <span class="identifiers"> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="10.5414/TEP23242" target="_blank" href="https://doi.org/10.5414/TEP23242"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="000241261700003" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000241261700003"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="33750414849" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-33750414849"> Scopus </a> </span> </span> </div> <div class="short-pub-prop-list"> <span class="short-pub-mtid"> Közlemény:1919903 </span> <span class="status-holder"><span class="status-data status-VALIDATED"> Egyeztetett </span></span> <span class="pub-core">Forrás Idéző </span> <span class="pub-type">Folyóiratcikk (Szakcikk ) </span> <!-- && !record.category.scientific --> <span class="pub-category">Tudományos</span> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 5</span> | Független: 5 | Függő: 0 | Nem jelölt: 0 | WoS jelölt: 3 | Scopus jelölt: 4 | WoS/Scopus jelölt: 5 | DOI jelölt: 3 </div> </div> </div> </div><div class="JournalArticle Publication long-list"> <div class="authors"> <img title="Forrásközlemény" style="float: left" src="/frontend/resources/grid/publication-core-icon.png"> <img title="Idézőközlemény" style="float: left" src="/frontend/resources/grid/publication-citation-icon.png"> <div class="autype autype0"> <span class="author-name" >Lengyel Zs ✉ </span> ; <span class="author-name" mtid="10028688"><a href="/gui2/?type=authors&mode=browse&sel=10028688" target="_blank">Lukács A (<span class="authorship-author-name">Lukács Anita</span> <span class="authorAux-mtmt"> toxikológia, megelőzés</span>) </a> </span> <span class="author-affil"><span title="Szegedi Tudományegyetem">SZTE</span>/<span title="Általános Orvostudományi Kar">ÁOK</span>/Népegészségtani Intézet</span> ; <span class="author-name" mtid="10028691"><a href="/gui2/?type=authors&mode=browse&sel=10028691" target="_blank">Szabó A (<span class="authorship-author-name">Szabó Andrea</span> <span class="authorAux-mtmt"> neurotoxikológia</span>) </a> </span> <span class="author-affil"><span title="Szegedi Tudományegyetem">SZTE</span>/<span title="Általános Orvostudományi Kar">ÁOK</span>/Népegészségtani Intézet</span> ; <span class="author-name" mtid="10010104"><a href="/gui2/?type=authors&mode=browse&sel=10010104" target="_blank">Nagymajtényi L (<span class="authorship-author-name">Nagymajtényi László</span> <span class="authorAux-mtmt"> Neurotoxikológia</span>) </a> </span> <span class="author-affil"><span title="Szegedi Tudományegyetem">SZTE</span>/<span title="Általános Orvostudományi Kar">ÁOK</span>/Népegészségtani Intézet</span> </div> </div> <div class="title"><a href="/gui2/?mode=browse¶ms=publication;1919903" target="_blank">General toxicity and neurotoxicity of lead and mercury, in combination with dimethoate, in rats after subchronic oral exposure.</a></div> <div> <span class="journal-title">TRACE ELEMENTS AND ELECTROLYTES</span> <span class="journal-issn">(<a target="_blank" href="https://portal.issn.org/resource/ISSN/0946-2104">0946-2104</a> <a target="_blank" href="https://portal.issn.org/resource/ISSN/0946-2104">0946-2104</a>)</span>: <span class="journal-volume">23</span> <span class="journal-issue">4</span> <span class="page"> pp 242-246 </span> <span class="year">(2006)</span> </div> <div class="pub-footer"> <span class="language" xmlns="http://www.w3.org/1999/html">Nyelv: Angol | </span> <span class="identifiers"> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="10.5414/TEP23242" target="_blank" href="https://doi.org/10.5414/TEP23242"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="000241261700003" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000241261700003"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="33750414849" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-33750414849"> Scopus </a> </span> </span> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 5</span> | Független: 5 | Függő: 0 | Nem jelölt: 0 | WoS jelölt: 3 | Scopus jelölt: 4 | WoS/Scopus jelölt: 5 | DOI jelölt: 3 </div> <div class="publication-citation"> <a target="_blank" href="/api/publication?cond=citations.related;eq;1919903&sort=publishedYear,desc&sort=title"> Idézett közlemények száma: 5 </a> </div> <div class="mtid"><span class="long-pub-mtid">Közlemény: 1919903</span> | <span class="status-data status-VALIDATED"> Egyeztetett </span> <span class="oldId">Régi azonosító: 1919903</span> | Forrás Idéző | <span class="type-subtype">Folyóiratcikk ( Szakcikk ) </span> | <span class="pub-category">Tudományos</span> | <span class="publication-sourceOfData">kézi felvitel</span> </div> <div class="lastModified">Utolsó módosítás: 2018.10.11. 16:39 WoS import (admin) </div> </div></div>
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Flow injection electrochemical hydride generation inductively coupled plasma time-of-flight mass spectrometry for the simultaneous determination of hydride forming elements and its application to the analysis of fresh water samples
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A flow injection (FI) method was developed using electrochemical hydride generation (EcHG) as a sample introduction system, coupled to an inductively coupled plasma time-of-flight mass spectrometer (ICP-TOFMS) for rapid and simultaneous determination of six elements forming hydrides (As, Bi, Ge, Hg, Sb and Se). A novel low volume electrolysis cell, especially suited for FI experiments was designed and the conditions for simultaneous electrochemical hydride generation (EcHG; electrolyte concentrations and flow rates, electrolysis voltage and current) as well as the ICP-TOFMS operational parameters (carrier gas flow rate, modulation pulse width (MPW)) for the simultaneous determination of 12 isotopes were optimized. The compromise operation parameters of the electrolysis were found to be 1.4 and 3mlmin-1 for the anolyte and catholyte flow rates, respectively, using 2M sulphuric acid. An optimum electrolysis current of 0.7A (16V) and an argon carrier gas flow rate of 0.91lmin-1 were chosen. A modulation pulse width of 5μs, which influences the sensitivity through the amount of ions being collected by the MS per single analytical cycle, provided optimum results for the detection of transient signals. The achieved detection limits were compared with those obtained by using FI in combination with conventional nebulization (FI-ICP-TOFMS); values for chemical hydride generation (FI-CHG-ICP-TOFMS) were taken from the literature. By using a 200μl sample loop absolute detection limits (3σ) in the range of 10-160pg for As, Bi, Ge, Hg, Sb and 1.1ng for Se and a precision of 4-8% for seven replicate injections of 20-100ngml-1 multielemental sample solutions were achieved. The analysis of a standard reference material (SRM) 1643d (NIST, "Trace Elements in Water") showed good agreement with the certified values for As and Sb. Se showed a drastic difference, which is probably due to the presence of hydride-inactive Se species in the sample. Recoveries better than 93% for Ge and Hg and 83.9% for Se were achieved on a spiked SRM sample. The developed method was successfully applied to the simultaneous multielemental determination of hydride forming elements in spring water samples originating from two different regions in Hungary. © 2002 Elsevier Science B.V. All rights reserved.
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<div class="JournalArticle Publication short-list"> <div class="authors"> <span class="author-name" > Bings, N H </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10002622"> <a href="/gui2/?type=authors&mode=browse&sel=10002622" target="_blank">Stefánka, Z</a> </span> <span class="author-type"> </span> ; <span class="author-name" > Rodríguez, Mallada S </span> <span class="author-type"> </span> </div ><div class="title"><a href="/gui2/?mode=browse¶ms=publication;1466225" mtid="1466225" target="_blank">Flow injection electrochemical hydride generation inductively coupled plasma time-of-flight mass spectrometry for the simultaneous determination of hydride forming elements and its application to the analysis of fresh water samples</a></div> <div class="pub-info"> <span class="journal-title">ANALYTICA CHIMICA ACTA</span> <span class="journal-volume">479</span> : <span class="journal-issue">2</span> <span class="page"> pp. 203-214. , 12 p. </span> <span class="year">(2003)</span> </div> <div class="pub-end"><div class="identifier-list"> <span class="identifiers"> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="10.1016/S0003-2670(02)01526-X" target="_blank" href="https://doi.org/10.1016/S0003-2670%2802%2901526-X"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="000181109800010" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000181109800010"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="0037430256" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-0037430256"> Scopus </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:black" title="10857264117563288150" target="_blank" href="http://scholar.Google.com/scholar?hl=en&lr=&cluster=10857264117563288150"> Google scholar </a> </span> </span> </div> <div class="short-pub-prop-list"> <span class="short-pub-mtid"> Közlemény:1466225 </span> <span class="status-holder"><span class="status-data status-APPROVED"> Nyilvános </span></span> <span class="pub-core">Forrás </span> <span class="pub-type">Folyóiratcikk (Szakcikk ) </span> <!-- && !record.category.scientific --> <span class="pub-category">Tudományos</span> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 60</span> | Független: 52 | Függő: 8 | Nem jelölt: 0 | WoS jelölt: 57 | Scopus jelölt: 57 | WoS/Scopus jelölt: 59 | DOI jelölt: 55 </div> </div> </div> </div><div class="JournalArticle Publication long-list"> <div class="authors"> <img title="Forrásközlemény" style="float: left" src="/frontend/resources/grid/publication-core-icon.png"> <div class="autype autype0"> <span class="author-name" >Bings N H </span> ; <span class="author-name" mtid="10002622"><a href="/gui2/?type=authors&mode=browse&sel=10002622" target="_blank">Stefánka Z (<span class="authorship-author-name">Stefánka Zsolt</span> <span class="authorAux-mtmt"> Analitikai kémia</span>) </a> </span> <span class="author-affil"><span title="MTA Energiatudományi Kutatóközpont">MTA EK</span>/Izotópkutató Intézet</span> ; <span class="author-name" >Rodríguez Mallada S </span> </div> </div> <div class="title"><a href="/gui2/?mode=browse¶ms=publication;1466225" target="_blank">Flow injection electrochemical hydride generation inductively coupled plasma time-of-flight mass spectrometry for the simultaneous determination of hydride forming elements and its application to the analysis of fresh water samples</a></div> <div> <span class="journal-title">ANALYTICA CHIMICA ACTA</span> <span class="journal-issn">(<a target="_blank" href="https://portal.issn.org/resource/ISSN/0003-2670">0003-2670</a> <a target="_blank" href="https://portal.issn.org/resource/ISSN/1873-4324">1873-4324</a>)</span>: <span class="journal-volume">479</span> <span class="journal-issue">2</span> <span class="page"> pp 203-214 </span> <span class="year">(2003)</span> </div> <div class="pub-footer"> <span class="language" xmlns="http://www.w3.org/1999/html">Nyelv: Angol | </span> <span class="identifiers"> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="10.1016/S0003-2670(02)01526-X" target="_blank" href="https://doi.org/10.1016/S0003-2670%2802%2901526-X"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="000181109800010" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000181109800010"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="0037430256" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-0037430256"> Scopus </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:black" title="10857264117563288150" target="_blank" href="http://scholar.Google.com/scholar?hl=en&lr=&cluster=10857264117563288150"> Google scholar </a> </span> </span> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 60</span> | Független: 52 | Függő: 8 | Nem jelölt: 0 | WoS jelölt: 57 | Scopus jelölt: 57 | WoS/Scopus jelölt: 59 | DOI jelölt: 55 </div> <div class="mtid"><span class="long-pub-mtid">Közlemény: 1466225</span> | <span class="status-data status-APPROVED"> Nyilvános </span> <span class="oldId">Régi azonosító: 1466225</span> | Forrás | <span class="type-subtype">Folyóiratcikk ( Szakcikk ) </span> | <span class="pub-category">Tudományos</span> | <span class="publication-sourceOfData">kézi felvitel</span> </div> <div class="lastModified">Utolsó módosítás: 2022.05.07. 17:58 Pécsi Éva (MTMT Közp 3, admin) </div> </div></div>