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The role of the solvation shell decomposition of alkali metal ions in their selective complexation by resorcinarene and its cavitand
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2-Methylresorcinarene and its methylene-bridged cavitand derivative as host compounds were investigated in selective
complexation of alkali metal ions as guests in methanol media by photoluminescence measurements. These host molecules
possess either flexible (2-methylresorcinarene) or rigid (cavitand) molecular skeleton. The Benesi–Hildebrand method and
the van’t Hoff theory have been applied to determine the stability constants and the thermodynamic parameters,
respectively. Considerable interactions between 2-methylresorcinarene and Liþ or Naþ ions have been observed while the
rigid cavitand derivative can interact only with Kþ or Csþ ions. Neither the complexes of 2-methylresorcinarene with Kþ or
Csþ nor those of the cavitand derivative with Liþ or Naþ ions are stable at room temperature in methanol media. Quantumchemical
investigations justified that only solvated Liþ and Naþ ions can form stable complexes with 2-methylresorcinarene
while unsolvated Kþ and Csþ ions form stable complexes with the methylene-bridged cavitand. These results highlight that
the stability of the guest solvation shell and its size could play a key role in the selectivity behaviour of host molecules.
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<div class="JournalArticle Publication short-list"> <div class="authors"> <span class="author-name" mtid="10025606"> <a href="/gui2/?type=authors&mode=browse&sel=10025606" target="_blank">Yin, Li</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10003539"> <a href="/gui2/?type=authors&mode=browse&sel=10003539" target="_blank">Zsolt, Csók</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10000480"> <a href="/gui2/?type=authors&mode=browse&sel=10000480" target="_blank">László, Kollár</a> </span> <span class="author-type"> </span> ; <span class="author-name" > Koichi, Iwata </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10025679"> <a href="/gui2/?type=authors&mode=browse&sel=10025679" target="_blank">Erzsébet, Szász</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10000668"> <a href="/gui2/?type=authors&mode=browse&sel=10000668" target="_blank">Sándor, Kunsági-Máté ✉</a> </span> <span class="author-type"> </span> </div ><div class="title"><a href="/gui2/?mode=browse¶ms=publication;2010539" mtid="2010539" target="_blank">The role of the solvation shell decomposition of alkali metal ions in their selective complexation by resorcinarene and its cavitand</a></div> <div class="pub-info"> <span class="journal-title">SUPRAMOLECULAR CHEMISTRY</span> <span class="journal-volume">24</span> : <span class="journal-issue">6</span> <span class="page"> pp. 374-378. , 5 p. </span> <span class="year">(2012)</span> </div> <div class="pub-end"><div class="identifier-list"> <span class="identifiers"> <span class="id identifier oa_PAY" title=" Fizetős "> <a style="color:blue" title="10.1080/10610278.2012.678358" target="_blank" href="https://doi.org/10.1080/10610278.2012.678358"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="000305486500002" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000305486500002"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="84862673662" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-84862673662"> Scopus </a> </span> </span> </div> <div class="short-pub-prop-list"> <span class="short-pub-mtid"> Közlemény:2010539 </span> <span class="status-holder"><span class="status-data status-VALIDATED"> Egyeztetett </span></span> <span class="pub-core">Forrás Idéző </span> <span class="pub-type">Folyóiratcikk (Szakcikk ) </span> <!-- && !record.category.scientific --> <span class="pub-category">Tudományos</span> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 8</span> | Független: 2 | Függő: 6 | Nem jelölt: 0 | WoS jelölt: 8 | Scopus jelölt: 8 | WoS/Scopus jelölt: 8 | DOI jelölt: 8 </div> </div> </div> </div><div class="JournalArticle Publication long-list"> <div class="authors"> <img title="Forrásközlemény" style="float: left" src="/frontend/resources/grid/publication-core-icon.png"> <img title="Idézőközlemény" style="float: left" src="/frontend/resources/grid/publication-citation-icon.png"> <div class="autype autype0"> <span class="author-name" mtid="10025606"><a href="/gui2/?type=authors&mode=browse&sel=10025606" target="_blank">Yin Li (<span class="authorship-author-name">Li Yin</span> <span class="authorAux-mtmt"> Physical Chemistry</span>) </a> </span> ; <span class="author-name" mtid="10003539"><a href="/gui2/?type=authors&mode=browse&sel=10003539" target="_blank">Zsolt Csók (<span class="authorship-author-name">Csók Zsolt</span> <span class="authorAux-mtmt"> Szervetlen kémia</span>) </a> </span> <span class="author-affil"><span title="Pécsi Tudományegyetem">PTE</span>/<span title="Természettudományi Kar">TTK</span>/<span title="Kémiai Intézet">KI</span>/Szervetlen Kémia Tanszék</span> ; <span class="author-name" mtid="10000480"><a href="/gui2/?type=authors&mode=browse&sel=10000480" target="_blank">László Kollár (<span class="authorship-author-name">Kollár László</span> <span class="authorAux-mtmt"> Homogén katalízis, koordinációs kémia</span>) </a> </span> <span class="author-affil"><span title="Pécsi Tudományegyetem">PTE</span>/<span title="Természettudományi Kar">TTK</span>/<span title="Kémiai Intézet">KI</span>/Szervetlen Kémia Tanszék; <span title="Pécsi Tudományegyetem">PTE</span>/<span title="Szentágothai János Kutatóközpont">SZKK</span>/Zöldkémia kutatócsoport</span> ; <span class="author-name" >Koichi Iwata </span> ; <span class="author-name" mtid="10025679"><a href="/gui2/?type=authors&mode=browse&sel=10025679" target="_blank">Erzsébet Szász (<span class="authorship-author-name">Szász Erzsébet</span> <span class="authorAux-mtmt"> Biokémia</span>) </a> </span> <span class="author-affil"><span title="Pécsi Tudományegyetem">PTE</span>/<span title="Természettudományi Kar">TTK</span>/<span title="Kémiai Intézet">KI</span>/Általános és Fizikai Kémia Tanszék</span> ; <span class="author-name" mtid="10000668"><a href="/gui2/?type=authors&mode=browse&sel=10000668" target="_blank">Sándor Kunsági-Máté ✉ (<span class="authorship-author-name">Kunsági-Máté Sándor</span> <span class="authorAux-mtmt"> Fizikai kémia</span>) </a> </span> <span class="author-affil"><span title="Pécsi Tudományegyetem">PTE</span>/<span title="Természettudományi Kar">TTK</span>/<span title="Kémiai Intézet">KI</span>/Általános és Fizikai Kémia Tanszék; <span title="Pécsi Tudományegyetem">PTE</span>/<span title="Szentágothai János Kutatóközpont">SZKK</span>/Zöldkémia kutatócsoport</span> </div> </div> <div class="title"><a href="/gui2/?mode=browse¶ms=publication;2010539" target="_blank">The role of the solvation shell decomposition of alkali metal ions in their selective complexation by resorcinarene and its cavitand</a></div> <div> <span class="journal-title">SUPRAMOLECULAR CHEMISTRY</span> <span class="journal-issn">(<a target="_blank" href="https://portal.issn.org/resource/ISSN/1061-0278">1061-0278</a> <a target="_blank" href="https://portal.issn.org/resource/ISSN/1029-0478">1029-0478</a>)</span>: <span class="journal-volume">24</span> <span class="journal-issue">6</span> <span class="page"> pp 374-378 </span> <span class="year">(2012)</span> </div> <div class="pub-footer"> <span class="language" xmlns="http://www.w3.org/1999/html">Nyelv: Angol | </span> <span class="identifiers"> <span class="id identifier oa_PAY" title=" Fizetős "> <a style="color:blue" title="10.1080/10610278.2012.678358" target="_blank" href="https://doi.org/10.1080/10610278.2012.678358"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="000305486500002" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000305486500002"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="84862673662" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-84862673662"> Scopus </a> </span> </span> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 8</span> | Független: 2 | Függő: 6 | Nem jelölt: 0 | WoS jelölt: 8 | Scopus jelölt: 8 | WoS/Scopus jelölt: 8 | DOI jelölt: 8 </div> <div class="publication-citation"> <a target="_blank" href="/api/publication?cond=citations.related;eq;2010539&sort=publishedYear,desc&sort=title"> Idézett közlemények száma: 9 </a> </div> <div class="mtid"><span class="long-pub-mtid">Közlemény: 2010539</span> | <span class="status-data status-VALIDATED"> Egyeztetett </span> <span class="oldId">Régi azonosító: 2010539</span> | Forrás Idéző | <span class="type-subtype">Folyóiratcikk ( Szakcikk ) </span> | <span class="pub-category">Tudományos</span> | <span class="publication-sourceOfData">kézi felvitel</span> </div> <div class="lastModified">Utolsó módosítás: 2023.09.02. 16:22 Milánkovics Róbert (PTE ÁOK admin 4) </div> </div></div>
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The interaction of phenol guest molecules with 2-methylresorcinarene and its methylene-bridged cavitand derivative has been investigated in methanol. The host molecules were selected according to the flexibility of their cavities by varying the conformational freedom of the molecular skeleton prior to molecular association. The results show stronger host-phenol interactions when the host molecule possesses a rigid molecular skeleton (i.e., cavitand) compared to that of the flexible resorcinarene with phenol. Although the enthalpy change associated with the molecular interactions was found to be the same in both cases, higher negative entropy change was obtained when the resorcinarene interacted with the phenol molecules at room temperature. As a result, stronger host-guest complexes are formed at room temperature when the host molecules, possessing a rigid molecular skeleton, participated in the complex formation. Furthermore, since the higher entropy change results in higher temperature-dependence of the interactions, the stability of the complexes formed with the flexible resorcinarene is smaller at higher temperature. These results highlight that the decreasing flexibility of the host molecular skeleton itself can determine the entropy change during the complexation process; therefore, the temperature dependence of the complex stabilities highly depends on the flexibility of the host's molecular skeleton. This information might contribute to the development of selective and sensitive sensor molecules toward phenol derivatives.
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<span class="long-book-mtid">Befoglaló: 3023537</span> <span class="oldId">Régi azonosító: 1750794</span> | <span class="oldId">Befoglaló: 3023537</span> Forrás | <span class="type-subtype">Egyéb konferenciaközlemény
( Konferenciaközlemény
)
</span>
| Tudományos
</span> | <span class="publication-sourceOfData">kézi felvitel</span>
</div>
<div class="lastModified">Utolsó módosítás: 2016.02.23. 11:38 Aggod Zsuzsa (MTMT 2-3, admin)
</div>
<pre class="comment" style="margin-top: 0; margin-bottom: 0;"><u>Megjegyzés</u>: Folyóirat nem található: The Proceedings of the International
Association of Theoretical and Applied Limnology
#Folyóirat nem található: International Association of
Theoretical and Applied Limnology
Füzet: 4
Kezdő oldal: 1995
Befejező oldal: 1999
Kötet: 27</pre>
</div><div class="comment">Folyóirat nem található: The Proceedings of the International
Association of Theoretical and Applied Limnology
#Folyóirat nem található: International Association of
Theoretical and Applied Limnology</div></div>
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A fényviszonyok, a nitrogénfölvétel és az elsődleges termelés kölcsönhatásai a Balaton eltérő trofitású tájain
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/api/publication/1750789
<div class="Thesis Publication short-list"> <div class="authors"> <span class="author-name" mtid="10025679"> <a href="/gui2/?type=authors&mode=browse&sel=10025679" target="_blank">Szász, Erzsébet</a> </span> <span class="author-type"> </span> </div > <div class="title"><a href="/gui2/?mode=browse¶ms=publication;1750789" mtid="1750789" target="_blank">A fényviszonyok, a nitrogénfölvétel és az elsődleges termelés kölcsönhatásai a Balaton eltérő trofitású tájain</a> 120 p.</div> <div class="pub-info"> <span class="publishedYear">Megjelenés/Fokozatszerzés éve: 1990</span> </div> <div class="pub-end"><div class="identifier-list"> <span class="identifiers"> </span> </div> <div class="short-pub-prop-list"> <span class="short-pub-mtid"> Közlemény:1750789 </span> <span class="status-holder"><span class="status-data status-APPROVED"> Nyilvános </span></span> <span class="pub-core">Forrás </span> <span class="pub-type">Disszertáció (Egyetemi doktor ) </span> <!-- && !record.category.scientific --> <span class="pub-category">Tudományos</span> </div> </div> </div><div class="Thesis Publication long-list">
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<img title="Forrásközlemény" style="float: left" src="/frontend/resources/grid/publication-core-icon.png">
<div class="autype autype0"> <span class="author-name" mtid="10025679"><a
href="/gui2/?type=authors&mode=browse&sel=10025679" target="_blank">Szász Erzsébet
(<span class="authorship-author-name">Szász Erzsébet</span>
<span class="authorAux-mtmt"> Biokémia</span>)
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<span class="author-affil"><span title="Pécsi Tudományegyetem">PTE</span>/<span title="Természettudományi Kar">TTK</span>/<span title="Kémiai Intézet">KI</span>/Általános és Fizikai Kémia Tanszék</span>
</div>
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<div class="title"><a href="/gui2/?mode=browse¶ms=publication;1750789" target="_blank">A fényviszonyok, a nitrogénfölvétel és az elsődleges termelés kölcsönhatásai a Balaton eltérő trofitású tájain</a></div> <div>
<span class="pageLength">120 p.</span>
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<div class="applicationYear">
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<div class="publishedYear">Megjelenés/Fokozatszerzés éve: 1990 </div>
<div class="pub-footer">
<span class="language" xmlns="http://www.w3.org/1999/html">Nyelv:
Magyar
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<span class="identifiers">
</span>
<div class="mtid"><span class="long-pub-mtid">Közlemény: 1750789</span>
| <span class="status-data status-APPROVED"> Nyilvános
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<span class="oldId">Régi azonosító: 1750789</span> |
Forrás
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( Egyetemi doktor
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| <span class="pub-category">Tudományos</span>
| <span class="publication-sourceOfData">kézi felvitel</span>
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<div class="lastModified">Utolsó módosítás: 2022.06.07. 22:25 Pécsi Éva (MTMT Közp 3, admin)
</div>
</div></div>