https://m2.mtmt.hu/ hun 2026-09-21 05:40 JournalArticle 36226846 VALIDATED true Cited by: 3; All Open Access; Gold Open Access; Green Open Access 0 false 2026-09-18T11:07:24.117+0000 2026-03-10T07:54:53.949+0000 2025-07-03T11:55:46.145+0000 true 10015206 Áncsán Gizella /api/admin/10015206 Admin Áncsán Gizella (SE admin) true 10015206 2026-09-18T10:33:02.953+0000 2025-09-10T12:18:31.045+0000 true 10071503 Szabó Regina /api/admin/10071503 Admin Szabó Regina (ELTE TTK admin 5) true 2025-12-25T03:09:29.593+0000 true 521 Szuper Admin /api/admin/521 Admin Szuper Admin (admin) true true false true 24 24 /api/publicationtype/24 PublicationType Folyóiratcikk 1 true 24 JournalArticle true 10000059 Article true 24 24 /api/publicationtype/24 PublicationType Folyóiratcikk 1 true 24 JournalArticle /api/subtype/10000059 Szakcikk SubType Szakcikk (Folyóiratcikk) 101 true 10000059 true 1 /api/category/1 Category Tudományos true 1 Magramane, Sabrina true true /api/journal/10022148 REVIEWED PHARMACEUTICS 1999-4923 true false 10022148 false 10022148 true 1999-4923 Journal FOREIGN 17 7 877 877 23 2025 Background/Objectives: This study investigates the impact of high humidity (25 °C, 75% relative humidity) on gelatin and hydroxypropyl methylcellulose (HPMC) capsules used in dry powder inhalers (DPIs), focusing on moisture dynamics, structural responses, and mechanical performance, with an emphasis on understanding how different capsule types respond to prolonged exposure to humid conditions. Methods: Capsules were exposed to controlled humidity conditions, and moisture uptake was measured via thermal analysis. Visual observations of silica bead color changes were performed to assess moisture absorption, while surface wettability was measured using the sessile drop method. Hardness testing, mechanical deformation, and puncture tests were performed to evaluate structural and mechanical changes. Positron annihilation lifetime spectroscopy (PALS) was used to analyze free volume expansion. Results: HPMC capsules exhibited rapid moisture uptake, attributed to their lower equilibrium moisture content and ability to rearrange dynamically, preventing brittleness. In contrast, gelatin capsules showed slower moisture absorption but reached higher equilibrium levels, resulting in plasticization and softening. Mechanical testing showed that HPMC capsules retained structural integrity with minimal deformation, while gelatin capsules became softer and exhibited reduced puncture resistance. Structural analysis revealed greater free volume expansion in HPMC capsules, consistent with their amorphous nature, compared with gelatin’s semi-crystalline matrix. Conclusions: HPMC capsules demonstrated superior humidity resilience, making them more suitable for protecting moisture-sensitive active pharmaceutical ingredients (APIs) in DPI formulations. These findings underline the importance of appropriate storage conditions, as outlined in the Summary of Product Characteristics, to ensure optimal capsule performance throughout patient use. true 2025 true true true false true false GOLD 2026-09-18 true https://doi.org/10.3390/pharmaceutics17070877 12 0 11 11 0 11 10 9 9 9 9 9 9 12 0 0 12 12 11 11 0 5 5 Folyóiratcikk Journal Article 24 11 Könyvrészlet Chapter in Book 25 0 Könyv Book 23 0 Egyéb konferenciaközlemény Conference paper 31 0 Egyéb konferenciakötet Conference proceedings 32 0 Oltalmi formák Protection forms 26 0 Disszertáció Thesis 28 1 Egyéb Miscellaneous 29 0 Alkotás Achievement 22 0 Kutatási adat Research data 33 0 Folyóiratcikk Journal Article 24 0 0 0 Könyvrészlet Chapter in Book 25 0 0 0 Könyv Book 23 0 0 0 Egyéb konferenciaközlemény Conference paper 31 0 0 0 Egyéb konferenciakötet Conference proceedings 32 0 0 0 Oltalmi formák Protection forms 26 0 0 0 Disszertáció Thesis 28 0 0 0 Egyéb Miscellaneous 29 0 0 0 Alkotás Achievement 22 0 0 0 Kutatási adat Research data 33 0 0 0 2025 0 3 3 3 3 2026 0 9 9 9 9 D1 false 10020626 false false false 2025-07-09T12:55:05.133+0000 Analitikai Kémiai Tanszék (ELTE / TTK / KI); Egyetemi Gyógyszertár Gyógyszerügyi Szervezési ... (SE / GYTK); Farmakológiai és Gyógyszerkutatás-fejlesztési K... (SE / KSZE); Gyógyszerészeti Intézet (SE / GYTK) 6 27 4 6 0 true Language 10002 /api/language/10002 Angol Angol English true 2 true PersonAuthorship 127120630 /api/authorship/127120630 Magramane, Sabrina [MAGRAMANE, Sabrina (Pharmacy), szerző] Gyógyszerészeti Intézet (SE / GYTK) 1 0.167 true false false Author 10071684 /api/author/10071684 MAGRAMANE Sabrina (Pharmacy) MAGRAMANE Sabrina true true Magramane Sabrina true false false AuthorshipType 1 /api/authorshiptype/1 Szerző 0 true 0 true false true PersonAuthorship 127120631 /api/authorship/127120631 Kállai-Szabó, Nikolett [Kállai-Szabó, Nikolett (Gyógyszertechnológia), szerző] Gyógyszerészeti Intézet (SE / GYTK); Farmakológiai és Gyógyszerkutatás-fejlesztési K... (SE / KSZE) 2 0.167 false false false Author 10020629 /api/author/10020629 Kállai-Szabó Nikolett (Gyógyszertechnológia) Kállai-Szabó Nikolett true 10020629 true Kállai-Szabó Nikolett true false false AuthorshipType 1 /api/authorshiptype/1 Szerző 0 true 0 true false true PersonAuthorship 127120632 /api/authorship/127120632 Farkas, Dóra [Farkas, Dóra (gyógyszertechnológia), szerző] Gyógyszerészeti Intézet (SE / GYTK) 3 0.167 false false false Author 10061229 /api/author/10061229 Farkas Dóra (gyógyszertechnológia) Farkas Dóra true 10061229 true Farkas Dóra true false false AuthorshipType 1 /api/authorshiptype/1 Szerző 0 true 0 true false true PersonAuthorship 127120633 /api/authorship/127120633 Süvegh, Károly [Süvegh, Károly (nukleáris tudományok), szerző] Analitikai Kémiai Tanszék (ELTE / TTK / KI) 4 0.167 false false false Author 10008061 /api/author/10008061 Süvegh Károly (nukleáris tudományok) Süvegh Károly true 10008061 true Süvegh Károly true false false AuthorshipType 1 /api/authorshiptype/1 Szerző 0 true 0 true false true PersonAuthorship 127120634 /api/authorship/127120634 Zelkó, Romána ✉ [Zelkó, Romána (Gyógyszertechnológia), szerző] Farmakológiai és Gyógyszerkutatás-fejlesztési K... (SE / KSZE); Egyetemi Gyógyszertár Gyógyszerügyi Szervezési ... (SE / GYTK) 5 0.167 false false true Author 10002587 /api/author/10002587 Zelkó Romána (Gyógyszertechnológia) Zelkó Romána true 10002587 true Zelkó Romána true false false AuthorshipType 1 /api/authorshiptype/1 Szerző 0 true 0 true false true PersonAuthorship 127120635 /api/authorship/127120635 Antal, István ✉ [Antal, István (Gyógyszertechnológia), szerző] Gyógyszerészeti Intézet (SE / GYTK); Farmakológiai és Gyógyszerkutatás-fejlesztési K... (SE / KSZE) 6 0.167 false true true Author 10020626 /api/author/10020626 Antal István (Gyógyszertechnológia) Antal István true 10020626 true Antal István true false false AuthorshipType 1 /api/authorshiptype/1 Szerző 0 true 0 true false true PublicationIdentifier 29554556 /api/publicationidentifier/29554556 DOI: 10.3390/pharmaceutics17070877 PlainSource 6 /api/publicationsource/6 DOI PublicationSourceType 10001 /api/publicationsourcetype/10001 DOI true true true DOI DOI https://doi.org/@@@ true true 6 true GOLD true IDENTICAL 10.3390/pharmaceutics17070877 https://doi.org/10.3390/pharmaceutics17070877 false true PublicationIdentifier 29715017 /api/publicationidentifier/29715017 WoS: 001540022300001 PlainSource 1 /api/publicationsource/1 WoS PublicationSourceType 10003 /api/publicationsourcetype/10003 Indexelő adatbázis false true true WoS WoS https://www.webofscience.com/wos/woscc/full-record/@@@ true true 1 true IDENTICAL 001540022300001 https://www.webofscience.com/wos/woscc/full-record/001540022300001 true true PublicationIdentifier 29698732 /api/publicationidentifier/29698732 Scopus: 105011712026 PlainSource 3 /api/publicationsource/3 Scopus PublicationSourceType 10003 /api/publicationsourcetype/10003 Indexelő adatbázis false true true Scopus Scopus http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-@@@ true true 3 true IDENTICAL 105011712026 http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-105011712026 true true PublicationIdentifier 29715018 /api/publicationidentifier/29715018 PubMed: 40733086 PlainSource 17 /api/publicationsource/17 PubMed PublicationSourceType 10003 /api/publicationsourcetype/10003 Indexelő adatbázis false true true PubMed PubMed http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?cmd=Retrieve&db=PubMed&list_uids=@@@&dopt=Abstract true true 17 true IDENTICAL 40733086 http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?cmd=Retrieve&db=PubMed&list_uids=40733086&dopt=Abstract true true SjrRating 11611771 /api/sjrrating/11611771 sjr:D1 (2025) Scopus - Pharmaceutical Science PHARMACEUTICS 1999-4923 18 0.1 journal RatingType 10002 /api/ratingtype/10002 sjr sjr true true ClassificationExternal 3003 /api/classificationexternal/3003 Scopus - Pharmaceutical Science true 3003 true D1 DIRECT true true Reference 66704043 /api/reference/66704043 1. 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(2025) PHARMACEUTICS 1999-4923 17 7<div class="JournalArticle Publication long-list"> <div class="authors"> <img title="Forrásközlemény" style="float: left" src="/frontend/resources/grid/publication-core-icon.png"> <img title="Idézőközlemény" style="float: left" src="/frontend/resources/grid/publication-citation-icon.png"> <div class="autype autype0"> <span class="author-name" mtid="10071684"><a href="/gui2/?type=authors&mode=browse&sel=10071684" target="_blank">Magramane Sabrina (<span class="authorship-author-name">MAGRAMANE Sabrina</span> <span class="authorAux-mtmt"> Pharmacy</span>) </a> </span> <span class="author-affil"><span title="Semmelweis Egyetem">SE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Gyógyszerészeti Intézet</span> ;&nbsp;&nbsp;&nbsp; <span class="author-name" mtid="10020629"><a href="/gui2/?type=authors&mode=browse&sel=10020629" target="_blank">Kállai-Szabó Nikolett (<span class="authorship-author-name">Kállai-Szabó Nikolett</span> <span class="authorAux-mtmt"> Gyógyszertechnológia</span>) </a> </span> <span class="author-affil"><span title="Semmelweis Egyetem">SE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Gyógyszerészeti Intézet; <span title="Semmelweis Egyetem">SE</span>/<span title="Központi Szervezeti Egységek (beleértve az Egyéb Szervezeti Egységeket)">KSZE</span>/Farmakológiai és Gyógyszerkutatás-fejlesztési Központ</span> ;&nbsp;&nbsp;&nbsp; <span class="author-name" mtid="10061229"><a href="/gui2/?type=authors&mode=browse&sel=10061229" target="_blank">Farkas Dóra (<span class="authorship-author-name">Farkas Dóra</span> <span class="authorAux-mtmt"> gyógyszertechnológia</span>) </a> </span> <span class="author-affil"><span title="Semmelweis Egyetem">SE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Gyógyszerészeti Intézet</span> ;&nbsp;&nbsp;&nbsp; <span class="author-name" mtid="10008061"><a href="/gui2/?type=authors&mode=browse&sel=10008061" target="_blank">Süvegh Károly (<span class="authorship-author-name">Süvegh Károly</span> <span class="authorAux-mtmt"> nukleáris tudományok</span>) </a> </span> <span class="author-affil"><span title="Eötvös Loránd Tudományegyetem">ELTE</span>/<span title="Természettudományi Kar">TTK</span>/<span title="Kémiai Intézet">KI</span>/Analitikai Kémiai Tanszék</span> ;&nbsp;&nbsp;&nbsp; <span class="author-name" mtid="10002587"><a href="/gui2/?type=authors&mode=browse&sel=10002587" target="_blank">Zelkó Romána ✉ (<span class="authorship-author-name">Zelkó Romána</span> <span class="authorAux-mtmt"> Gyógyszertechnológia</span>) </a> </span> <span class="author-affil"><span title="Semmelweis Egyetem">SE</span>/<span title="Központi Szervezeti Egységek (beleértve az Egyéb Szervezeti Egységeket)">KSZE</span>/Farmakológiai és Gyógyszerkutatás-fejlesztési Központ; <span title="Semmelweis Egyetem">SE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Egyetemi Gyógyszertár Gyógyszerügyi Szervezési Intézet</span> ;&nbsp;&nbsp;&nbsp; <span class="author-name" mtid="10020626"><a href="/gui2/?type=authors&mode=browse&sel=10020626" target="_blank">Antal István ✉ (<span class="authorship-author-name">Antal István</span> <span class="authorAux-mtmt"> Gyógyszertechnológia</span>) </a> </span> <span class="author-affil"><span title="Semmelweis Egyetem">SE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Gyógyszerészeti Intézet; <span title="Semmelweis Egyetem">SE</span>/<span title="Központi Szervezeti Egységek (beleértve az Egyéb Szervezeti Egységeket)">KSZE</span>/Farmakológiai és Gyógyszerkutatás-fejlesztési Központ</span> </div> </div> <div class="title"><a href="/gui2/?mode=browse&params=publication;36226846" target="_blank">Comparative Evaluation of Gelatin and HPMC Inhalation Capsule Shells Exposed to Simulated Humidity Conditions</a></div> <div> <span class="journal-title">PHARMACEUTICS</span> <span class="journal-issn">( <a target="_blank" href="https://portal.issn.org/resource/ISSN/1999-4923">1999-4923</a>)</span>: <span class="journal-volume">17</span> <span class="journal-issue">7</span> <span class="page"> Paper 877. 23 p. </span> <span class="year">(2025)</span> </div> <div class="pub-footer"> <span class="language" xmlns="http://www.w3.org/1999/html">Nyelv: Angol | </span> <span class="identifiers"> <span class="id identifier oa_GOLD" title=" Gold "> <a style="color:blue" title="10.3390/pharmaceutics17070877" target="_blank" href="https://doi.org/10.3390/pharmaceutics17070877"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="001540022300001" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/001540022300001"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="105011712026" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-105011712026"> Scopus </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="40733086" target="_blank" href="http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?cmd=Retrieve&db=PubMed&list_uids=40733086&dopt=Abstract"> PubMed </a> </span> </span> <OnlyViewableByAuthor><div class="ratings"> <div class="journal-subject">Folyóirat szakterülete: Scopus - Pharmaceutical Science&nbsp;&nbsp;&nbsp;SJR indikátor:&nbsp;D1</div> </div></OnlyViewableByAuthor> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 12</span> | Független: 12 | Függő: 0 | Nem jelölt: 0 | WoS jelölt: 9 | Scopus jelölt:&nbsp;9 | WoS/Scopus jelölt:&nbsp;9 | DOI jelölt:&nbsp;10 </div> <div class="publication-citation"> <a target="_blank" href="/api/publication?cond=citations.related;eq;36226846&sort=publishedYear,desc&sort=title"> Idézett közlemények száma: 5 </a> </div> <div class="mtid"><span class="long-pub-mtid">Közlemény: 36226846</span> | <span class="status-data status-VALIDATED"> Egyeztetett </span> Forrás Idéző | <span class="type-subtype">Folyóiratcikk ( Szakcikk ) </span> | <span class="pub-category">Tudományos</span> | <span class="publication-sourceOfData">WOS TAGGED</span> </div> <div class="lastModified">Utolsó módosítás: 2026.03.10. 08:54 Áncsán Gizella (SE admin) </div> <pre class="comment" style="margin-top: 0; margin-bottom: 0;"><u>Megjegyzés</u>: Cited by: 3; All Open Access; Gold Open Access; Green Open Access</pre> </div></div>