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A linear relationship between the sigma(Hammett) and Sn-119 NMR chemical shift was found due to the electron-withdrawing and electron-donating groups. H-1 and Sn-119 NMR titration experiments with DCI were carried in CD3OD solution to estimate the stability of the complexes and study the equilibrium between four- and five-coordinate complexes. The most basic sites for protonation were determined by analysis of the electrostatic potential by theoretical calculations. (C) 2020 Elsevier B.V. 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