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Use of copper-polyethylenimine nanoparticles (nCu-PEI) as a catalyst, with H2O2 as a radical source, is demonstrated for the degradation of 5-fluorouracil (5-FU). Optimal reaction conditions were found, and 5-FU was degraded completely within 24 h, following first-order kinetics with a reaction rate of 0.003 min(-1). Stoichiometric formation of F- was shown with the degradation of 5-FU. Substitution of uracil with other halogen groups led to a decrease in the reaction rate. By comparison, the rate of 5-Chlorouracil degradation was 0.002 min(-1) and that of 5-Bromouracil degradation was 0.001 min(-1). Stoichiometric formation of halogens was observed. A similar trend of decreasing reaction rate was found for the degradation of uracil in the presence of halogen salts. 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