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Synthesis of 1,2,3,4-tetrahydroisoquinoline-1-carboxylic Acid Derivatives Via Ugi Reactions
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The three-component Ugi reactions of 3,4-dihydroisoquinolines, isocyanides and acids furnished 2-acyl-N-substituted-1,2,3,4-tetrahydroisoquinoline-1-carboxamides in moderate to good yields. Chiral, nonracemic acids induced only poor diastercoselectivities in the condensations. Hydrolysis of the Ugi carboxamides gave the corresponding 1,2,3,4-tetrahydroisoquinoline-1-carboxylic acids, which due to their ready ability to undergo racemization, were obtained as racemic mixtures or with low enantiomeric excesses.
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/api/publication/1083281
<div class="JournalArticle Publication short-list"> <div class="authors"> <span class="author-name" mtid="10029683"> <a href="/gui2/?type=authors&mode=browse&sel=10029683" target="_blank">Schuster, I</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10028825"> <a href="/gui2/?type=authors&mode=browse&sel=10028825" target="_blank">Sztojkov, Ivanov A</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="10002383"> <a href="/gui2/?type=authors&mode=browse&sel=10002383" target="_blank">Lazar, L</a> </span> <span class="author-type"> </span> ; <span class="author-name" mtid="1381350"> <a href="/gui2/?type=authors&mode=browse&sel=1381350" target="_blank">Fulop, F ✉</a> </span> <span class="author-type"> </span> </div ><div class="title"><a href="/gui2/?mode=browse¶ms=publication;1083281" mtid="1083281" target="_blank">Synthesis of 1,2,3,4-tetrahydroisoquinoline-1-carboxylic Acid Derivatives Via Ugi Reactions</a></div> <div class="pub-info"> <span class="journal-title">LETTERS IN ORGANIC CHEMISTRY</span> <span class="journal-volume">4</span> : <span class="journal-issue">2</span> <span class="page"> pp. 102-108. , 7 p. </span> <span class="year">(2007)</span> </div> <div class="pub-end"><div class="identifier-list"> <span class="identifiers"> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="10.2174/157017807780414226" target="_blank" href="https://doi.org/10.2174/157017807780414226"> DOI </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="000246567100005" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000246567100005"> WoS </a> </span> <span class="id identifier oa_none" title="none"> <a style="color:blue" title="34247860900" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-34247860900"> Scopus </a> </span> </span> </div> <div class="short-pub-prop-list"> <span class="short-pub-mtid"> Közlemény:1083281 </span> <span class="status-holder"><span class="status-data status-VALIDATED"> Egyeztetett </span></span> <span class="pub-core">Forrás Idéző </span> <span class="pub-type">Folyóiratcikk (Szakcikk ) </span> <!-- && !record.category.scientific --> <span class="pub-category">Tudományos</span> <div class="publication-citation" style="margin-left: 0.5cm;"> <span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 9</span> | Független: 8 | Függő: 1 | Nem jelölt: 0 | WoS jelölt: 9 | Scopus jelölt: 9 | WoS/Scopus jelölt: 9 | DOI jelölt: 9 (Nem nyilvános: 2) </div> </div> </div> </div><div class="JournalArticle Publication long-list">
<div class="authors">
<img title="Forrásközlemény" style="float: left" src="/frontend/resources/grid/publication-core-icon.png">
<img title="Idézőközlemény" style="float: left" src="/frontend/resources/grid/publication-citation-icon.png">
<div class="autype autype0"> <span class="author-name" mtid="10029683"><a
href="/gui2/?type=authors&mode=browse&sel=10029683" target="_blank">Schuster I
(<span class="authorship-author-name">Schuster Ildikó</span>
<span class="authorAux-mtmt"> Kémia</span>)
</a>
</span>
<span class="author-affil"><span title="Szegedi Tudományegyetem">SZTE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Gyógyszerkémiai Intézet</span>
;
<span class="author-name" mtid="10028825"><a
href="/gui2/?type=authors&mode=browse&sel=10028825" target="_blank">Sztojkov Ivanov A
(<span class="authorship-author-name">Sztojkov-Ivanov Anita</span>
<span class="authorAux-mtmt"> Kromatográfia</span>)
</a>
</span>
;
<span class="author-name" mtid="10002383"><a
href="/gui2/?type=authors&mode=browse&sel=10002383" target="_blank">Lazar L
(<span class="authorship-author-name">Lázár László</span>
<span class="authorAux-mtmt"> Szerves kémia, gyógyszerkémia</span>)
</a>
</span>
<span class="author-affil"><span title="Szegedi Tudományegyetem">SZTE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Gyógyszerkémiai Intézet</span>
;
<span class="author-name" mtid="1381350"><a
href="/gui2/?type=authors&mode=browse&sel=1381350" target="_blank">Fulop F ✉
(<span class="authorship-author-name">Fülöp Ferenc</span>
<span class="authorAux-mtmt"> Kémia</span>)
</a>
</span>
<span class="author-affil"><span title="Szegedi Tudományegyetem">SZTE</span>/<span title="Gyógyszerésztudományi Kar">GYTK</span>/Gyógyszerkémiai Intézet</span>
</div>
</div>
<div class="title"><a href="/gui2/?mode=browse¶ms=publication;1083281" target="_blank">Synthesis of 1,2,3,4-tetrahydroisoquinoline-1-carboxylic Acid Derivatives Via Ugi Reactions</a></div> <div> <span class="journal-title">LETTERS IN ORGANIC CHEMISTRY</span>
<span class="journal-issn">(<a target="_blank" href="https://portal.issn.org/resource/ISSN/1570-1786">1570-1786</a> <a target="_blank" href="https://portal.issn.org/resource/ISSN/1875-6255">1875-6255</a>)</span>:
<span class="journal-volume">4</span> <span class="journal-issue">2</span>
<span class="page">
pp 102-108
</span> <span class="year">(2007)</span>
</div>
<div class="pub-footer">
<span class="language" xmlns="http://www.w3.org/1999/html">Nyelv:
Angol
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<span class="identifiers">
<span class="id identifier oa_none" title="none">
<a style="color:blue" title="10.2174/157017807780414226" target="_blank" href="https://doi.org/10.2174/157017807780414226">
DOI
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</span>
<span class="id identifier oa_none" title="none">
<a style="color:blue" title="000246567100005" target="_blank" href="https://www.webofscience.com/wos/woscc/full-record/000246567100005">
WoS
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<span class="id identifier oa_none" title="none">
<a style="color:blue" title="34247860900" target="_blank" href="http://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-34247860900">
Scopus
</a>
</span>
</span>
<div class="publication-citation" style="margin-left: 0.5cm;">
<span title="Nyilvános idézőközlemények összesen, említések nélkül" class="citingPub-count">Nyilvános idéző összesen: 9</span>
| Független: 8
| Függő: 1
| Nem jelölt: 0
| WoS jelölt: 9
| Scopus jelölt: 9
| WoS/Scopus jelölt: 9
| DOI jelölt: 9
(Nem nyilvános: 2)
</div>
<div class="publication-citation">
<a target="_blank" href="/api/publication?cond=citations.related;eq;1083281&sort=publishedYear,desc&sort=title">
Idézett közlemények száma: 4
</a>
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<div class="mtid"><span class="long-pub-mtid">Közlemény: 1083281</span>
| <span class="status-data status-VALIDATED"> Egyeztetett
</span>
<span class="oldId">Régi azonosító: 1083281</span> |
Forrás Idéző
| <span class="type-subtype">Folyóiratcikk
( Szakcikk
)
</span>
| <span class="pub-category">Tudományos</span>
| <span class="publication-sourceOfData">WOS</span>
</div>
<div class="lastModified">Utolsó módosítás: 2022.07.13. 13:06 Áts József (admin)
</div>
<pre class="comment" style="margin-top: 0; margin-bottom: 0;"><u>Megjegyzés</u>: Univ Szeged, Inst Pharmaceut Chem, H-6701 Szeged, Hungary.</pre>
</div></div>